HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
O-Methylhydroxylamine → N-Benzyloxy-3-(2-chloro-4-iodo-phenylamino)-isonicotinamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | O-Methylhydroxylamine | HCID 4113 | — |
| Edukt | 3-[(2-Chloro-4-iodophenyl)amino]isonicotinic acid | HCID 57649651 | — |
| Produkt | N-Benzyloxy-3-(2-chloro-4-iodo-phenylamino)-isonicotinamide | HCID 11677348 | — |
Reaktionsschritte
N-Benzyloxy-3-(2-chloro-4-iodo-phenylamino)-isonicotinamide was synthesized according to the procedure for General Method 1, outlined above, starting with 0.25 mmol of 3-[(2-chloro-4-iodophenyl)amino]isonicotinic acid (intermediate 2) and 0.36 mmol of O-methyl-hydroxylamine. LC/MS [10.01 min; 480 (M+1)]
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08198457B2 |
| Quelldatensatz | uspto-grants-2012_06 |
| ORD ID | ord-b21cd1f2257a4ea7a4bd46dfbb209f22 |
| Quellennotiz | uspto-grants-2012_06 |