m-Tolylhydrazine → HCID 11662626, compound

HRID 218949Notes

Reaction equation

HRID 218949 reaction equation
[F:1][C:2]1[CH:7]=[C:6]([I:8])[CH:5]=[CH:4][C:3]=1[NH:9][C:10]1[CH:18]=[N:17][CH:16]=[CH:15][C:11]=1[C:12]([OH:14])=O.[CH3:19][C:20]1[CH:21]=[C:22]([NH:26][NH2:27])[CH:23]=[CH:24][CH:25]=1>>[F:1][C:2]1[CH:7]=[C:6]([I:8])[CH:5]=[CH:4][C:3]=1[NH:9][C:10]1[CH:18]=[N:17][CH:16]=[CH:15][C:11]=1[C:12]([NH:27][NH:26][C:22]1[CH:23]=[CH:24][CH:25]=[C:20]([CH3:19])[CH:21]=1)=[O:14]

Participants

3

Reactant 2

HCID 68308m-TolylhydrazineHCID 590267913-((2-Fluoro-4-iodophenyl)amino)isonicotinic acid2×

Product 1

HCID 11662626HCID 11662626, compound

Procedure

was synthesized according to the procedure for General Method 1, outlined above, starting with 0.44 mmol of 3-[(2-fluoro-4-iodophenyl)amino]isonicotinic acid (intermediate 1) and 0.63 mmol of 3-methyl-phenylhydrazine. LC/MS [6.05 min; 463 (M+1)]

Workup

  1. customwas synthesized
  2. customLC/MS [6.05 min; 463 (M+1)]

Sources & evidence

ORD record
ord-faf84492293342ac97c919955c31b2d6
Source dataset
uspto-grants-2012_06
Patent number
US08198457B2

Reaction notes

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