HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Benzylhydroxylamine → N-(benzyloxy)-3-[(2-fluoro-4-iodophenyl)amino]isonicotinamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Benzylhydroxylamine | HCID 102313 | — |
| Reactant | 3-((2-Fluoro-4-iodophenyl)amino)isonicotinic acid | HCID 59026791 | — |
| Product | N-(benzyloxy)-3-[(2-fluoro-4-iodophenyl)amino]isonicotinamide | HCID 11503610 | — |
Reaction Steps
N-(benzyloxy)-3-[(2-fluoro-4-iodophenyl)amino]isonicotinamide was synthesized according to the procedure for General Method 1, outlined above, starting with 0.5 mmol of 3-[(2-fluoro-4-iodophenyl)amino]isonicotinic acid (intermediate 1) and 0.72 mmol of O-benzyl-hydroxylamine. LC/MS [9.50 min; 464 (M+1)]
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08198457B2 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-99bbd5498b7643c5a726f329f9de5cf6 |
| Source note | uspto-grants-2012_06 |