Ammonia → HCID 131727631, compound

HRID 218972Notes

Reaction equation

HRID 218972 reaction equation
[C:1]([C:5]([C:8]([O:11][CH2:12][C:13]([C:16]([OH:18])=[O:17])([F:15])[F:14])([F:10])[F:9])([F:7])[F:6])([F:4])([F:3])[F:2].[NH3:19].[OH-].[Na+]>>[C:1]([C:5]([C:8]([O:11][CH2:12][C:13]([C:16]([O-:18])=[O:17])([F:15])[F:14])([F:9])[F:10])([F:7])[F:6])([F:4])([F:3])[F:2].[NH4+:19]

Participants

4

Reactant 3

HCID 222AmmoniaHCID 14798Sodium HydroxideHCID 714186562,2-Difluoro-3-(heptafluoropropoxy)propanoic acid

Product 1

HCID 131727631HCID 131727631, compound

Procedure

An aqueous solution of CF3CF2CF2OCH2CF2COONH4 (20.2% by mass) was prepared in the same manner as in Synthesis Example 1 except that the CF3CF2CF2OCH2CF2COOH prepared in Synthesis Example 1 was neutralized to pH 7 using aqueous ammonia in lieu of the aqueous solution of sodium hydroxide.

Workup

  1. customprepared in Synthesis Example 1

Sources & evidence

ORD record
ord-b608d4f40f7c4d5b8b25e64aa533e41a
Source dataset
uspto-grants-2012_06
Patent number
US08198480B2

Reaction notes

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