Ammonia → HCID 131727632, compound

HRID 218974Notes

Reaction equation

HRID 218974 reaction equation
[C:1]([C:5]([C:8]([C:11]([O:14][CH2:15][C:16]([C:19]([OH:21])=[O:20])([F:18])[F:17])([F:13])[F:12])([F:10])[F:9])([F:7])[F:6])([F:4])([F:3])[F:2].[NH3:22].[OH-].[Na+]>>[C:1]([C:5]([C:8]([C:11]([O:14][CH2:15][C:16]([C:19]([O-:21])=[O:20])([F:18])[F:17])([F:12])[F:13])([F:10])[F:9])([F:7])[F:6])([F:4])([F:3])[F:2].[NH4+:22]

Participants

4

Reactant 3

HCID 222AmmoniaHCID 14798Sodium HydroxideHCID 714186542,2-Difluoro-3-(nonafluorobutoxy)propanoic acid

Product 1

HCID 131727632HCID 131727632, compound

Procedure

An aqueous solution of CF3CF2CF2CF2OCH2CF2COONH4 was prepared in the same manner as in Synthesis Example 1 except that the CF3CF2CF2CF2OCH2CF2COOH prepared in Synthesis Example 3 was neutralized to pH 7 using aqueous ammonia in lieu of the aqueous solution of sodium hydroxide.

Workup

  1. customprepared in Synthesis Example 3

Sources & evidence

ORD record
ord-3198430694dd464e8711a1c3535e8cef
Source dataset
uspto-grants-2012_06
Patent number
US08198480B2

Reaction notes

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