Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
tert-Butyl Formate → Tert-butyl 5-bromospiro[indoline-3,4'-piperidine]-1'-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | tert-Butyl Formate | HCID 61207 | — |
| 반응물 | Tert-butyl 5-bromospiro[indole-3,4'-piperidine]-1'-carboxylate | HCID 68758388 | — |
| 생성물 | Tert-butyl 5-bromospiro[indoline-3,4'-piperidine]-1'-carboxylate | HCID 49760955 | — |
반응 단계
Tert-butyl 5-bromospiro[indoline-3,4′-piperidine]-1′-carboxylate was prepared by the procedures described in Example 1, Step 2, substituting tert-butyl 5-chlorospiro[indole-3,4′-piperidine]-1′-carboxylate with tert-butyl 5-bromospiro[indole-3,4′-piperidine]-1′-carboxylate. LCMS (APCI+) m/z 267, 269 [M+H-Boc]+; Rt=3.89 min.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08324221B2 |
| 출처 데이터셋 | uspto-grants-2012_12 |
| ORD ID | ord-9c1e16cb46d244f6a6002b4da00cf960 |
| 출처 메모 | uspto-grants-2012_12 |