HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → HCID 86655369, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | Potassium thiocyanate | HCID 516872 | — |
| Reactant | N-[3-(4-aminophenoxy)-4-methoxyphenyl]-3-(1-cyano-1-methylethyl)benzamide | HCID 67312983 | — |
| Product | HCID 86655369 | HCID 86655369 | 80% |
Reaction Steps
Using N-[3-(4-aminophenoxy)-4-methoxyphenyl]-3-(1-cyano-1-methylethyl)benzamide (1.10 g, 2.74 mmol), potassium thiocyanate (0.97 g, 10.0 mmol) and bromine (0.60 g, 3.75 mmol), and in the same manner as in Example A18(iv), the title compound (1.00 g, 80%) was obtained as a yellow powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08324395B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-59401b161f2c4f4dadf50fdf4103e127 |
| Source note | uspto-grants-2012_12 |