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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2190430Generated: November 1, 2026

Bromine → HCID 86655379, compound

https://huagongshe.com/reaction/2190430

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBromineHCID 24408—
ReactantPotassium thiocyanateHCID 516872—
ReactantHCID 67312567HCID 67312567—
ProductHCID 86655379HCID 8665537979.3%

Reaction Steps

Using 3-(4-aminophenoxy)-N-[3-(trifluoromethyl)phenyl]benzamide (2.45 g, 6.58 mmol), potassium thiocyanate (1.94 g, 20.0 mmol) and bromine (1.20 g, 7.50 mmol), and in the same manner as in Example A25(v), the title compound (2.24 g, 79%) was obtained as a pale-yellow powder.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08324395B2
Source datasetuspto-grants-2012_12
ORD IDord-6e4b2dbce74745198aab76e7a9f5addf
Source noteuspto-grants-2012_12