Methanol → HCID 67313230, compound

Participants

Reaction Steps

To a solution of methyl 3-[3-(benzyloxy)-4-nitrophenoxy]benzoate (19.1 g, 50.4 mmol) in ethyl acetate (50 mL) were added methanol (80 mL) and 10% palladium-carbon (2.31 g), and the mixture was vigorously stirred at room temperature for 20 hr under a hydrogen atmosphere. 10% Palladium-carbon was filtered off, and the filtrate was concentrated under reduced pressure to give the title compound (13.1 g) as a brown syrup.

Provenance & Evidence