HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoic acid, 3-amino-, methyl ester → HCID 26240629, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoic acid, 3-amino-, methyl ester | HCID 78274 | — |
| Reactant | 6-Chloronicotinoyl Chloride | HCID 2782165 | — |
| Reactant | 6-chloro-N-(4-iodo-3-methyl-phenyl)-nicotinamide | HCID 59318138 | — |
| Product | HCID 26240629 | HCID 26240629 | — |
Reaction Steps
3-[(6-Chloro-pyridine-3-carbonyl)-amino]-benzoic acid methyl ester was prepared from 3-amino-benzoic acid methyl ester and 6-chloronicotinoyl chloride following a procedure similar to the one described in the synthesis of 6-chloro-N-(4-iodo-3-methyl-phenyl)-nicotinamide, above. The product was isolated after precipitation out of a small volume of CH2Cl2 with hexanes. HRMS m/z calcd for C14H11N2O3Cl [M+H]+: 291.0531. Found: 291.0531.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08324385B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-fb953f69b45944a5ad0173d74c51d97b |
| Source note | uspto-grants-2012_12 |