HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Nitro-4-propylphenol → 2-amino-4-propylphenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Nitro-4-propylphenol | HCID 240553 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 2-amino-4-propylphenol | HCID 721138 | 93.2% |
Reaction Steps
A mixture of 6.65 g of 4-propyl-2-nitrophenol, 55 ml of ethyl acetate and 1.0 g of 5% palladium on carbon was stirred under about one atmosphere of hydrogen at room temperature for two hours. The mixture was filtered through Celite™. The filtrate was concentrated under reduced pressure to give 5.17 g of 2-amino-4-propylphenol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08324387B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-4467fe972d954b5cbda6fe3a44eef9f5 |
| Source note | uspto-grants-2012_12 |