HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57840754, compound → HCID 57840753, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57840754 | HCID 57840754 | — |
| Catalyst | Manganese dioxide | HCID 14801 | — |
| Product | HCID 57840753 | HCID 57840753 | 58.8% |
Reaction Steps
According to the General Procedure B, MnO2 (1.63 g, 18.70 mmol) and 2-(3-ethoxy-4-methoxyphenyl)-1,4-pentadien-3-ol (200 mg, 0.85 mmol) are converted to give after workup and chromatography (SiO2, PE/EE=2:1, Rf=0.40) the title compound (110 mg, 0.50 mmol) as a yellow oil; C14H16O3 (232.27).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08324404B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-d1c521caac4d4407887141309d2e507e |
| Source note | uspto-grants-2012_12 |