Cyclohexane, (bromomethyl)- → HCID 67523816, compound

HRID 2190928Notes

Reaction equation

HRID 2190928 reaction equation
[OH:1][C:2]1[CH:3]=[CH:4][C:5]2[O:10][C:9]([CH3:12])([CH3:11])[O:8][C:7](=[O:13])[C:6]=2[CH:14]=1.BrC[CH:17]1[CH2:22][CH2:21][CH2:20][CH2:19][CH2:18]1>>[CH2:21]([O:1][C:2]1[CH:3]=[CH:4][C:5]2[O:10][C:9]([CH3:11])([CH3:12])[O:8][C:7](=[O:13])[C:6]=2[CH:14]=1)[CH2:22][CH2:17][CH2:18][CH2:19][CH3:20]

Participants

3

Reactant 2

HCID 137636Cyclohexane, (bromomethyl)-HCID 67421272HCID 67421272, compound

Product 1

HCID 67523816HCID 67523816, compound

Procedure

The title compound was prepared from 6-hydroxy-2,2-dimethyl-benzo[1,3]dioxin-4-one (example 38-a) and (bromomethyl)cyclohexane under conditions analogous to experimental example 38-b, to give the desired product as a white solid. MS: (+) m/z 279.16 (M+1)

Sources & evidence

ORD record
ord-332bb27e2eb54fb881c3938917b61443
Source dataset
uspto-grants-2012_12
Patent number
US08324405B2

Reaction notes

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