Isopropyl iodide → HCID 67523696, compound

HRID 2190930Notes

Reaction equation

HRID 2190930 reaction equation
[OH:1][C:2]1[CH:3]=[CH:4][C:5]2[O:10][C:9]([CH3:12])([CH3:11])[O:8][C:7](=[O:13])[C:6]=2[CH:14]=1.I[CH:16]([CH3:18])[CH3:17]>>[CH:16]([O:1][C:2]1[CH:3]=[CH:4][C:5]2[O:10][C:9]([CH3:11])([CH3:12])[O:8][C:7](=[O:13])[C:6]=2[CH:14]=1)([CH3:18])[CH3:17]

Participants

3

Reactant 2

HCID 6362Isopropyl iodideHCID 67421272HCID 67421272, compound

Product 1

HCID 67523696HCID 67523696, compound

Procedure

The title compound was prepared from 6-hydroxy-2,2-dimethyl-benzo[1,3]dioxin-4-one (example 38-a) and 2-iodopropane under conditions analogous to experimental example 38-b, to give the desired product as a white solid. MS: (+) m/z 237.12 (M+1)

Sources & evidence

ORD record
ord-2034d1be13924310ad27b4431758f9c8
Source dataset
uspto-grants-2012_12
Patent number
US08324405B2

Reaction notes

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