HRID2191057

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CCOP(=O)(/C=C/[C@@H]1C[C@@H](OC(=O)c2ccccc2)[C@H](n2nnc3c(N)ncnc32)O1)OCC

HCID59289341

未命名化合物

结构：CC(=O)Nc1nc2c(ncn2C2OC(C=CP(=O)(O)O)CC2OC(=O)c2ccccc2)c(=O)[nH]1

HCID136381446

未命名化合物

PRODUCTS

生成物

结构：Nc1ncnc2c1nnn2[C@@H]1O[C@H](/C=C/P(=O)(O)O)C[C@H]1O

HCID25152957

未命名化合物

收率 76.2%

PROCEDURE

实验过程

Compound 38.2 (60 mg, 68% yield) was synthesized from compound 38.1 (115 mg, 0.24 mmol) using the procedure described for the preparation of compound 9.10. 1H NMR (D2O, 300 MHz): δ 2.31-2.55 (m, 2H), 4.78-4.98 (m, 2H), 5.78-5.88 (m, 1H), 5.94-6.08 (m, 1H), 6.23 (s, 1H). 31PNMR: 9.20 ppm. LRMS C10H13N6O5P requires 327.1. Found 327.0.