Methanol → HCID 68958545, compound

Participants

Reaction Steps

To a mixed solution of methanol 18 mL and ethyl acetate 18 mL of tert-butyl 4-(3-(tert-butoxycarbonyl)oxyphenyl)-2-nitrobenzoate 3.5 g was added 5% palladium-carbon 0.70 g, and it was stirred under hydrogen atmosphere at room temperature for 3 hours and 30 minutes. The solvent was removed under reduced pressure after insoluble matter was filtrated to give tert-butyl 2-amino-4-(3-(tert-butoxycarbonyl)oxyphenyl)benzoate 3.2 g of yellow oil.

Provenance & Evidence