Methanol → HCID 57667938, compound

Participants

Reaction Steps

To a mixed solution of methanol 2.0 mL and ethyl acetate 1.0 mL of 2-(2-nitroanilino)-4-phenethylbenzoic acid 20 mg was added 5% palladium-carbon 8 mg, and it was stirred under hydrogen atmosphere at room temperature for 3 hours. Insoluble matter was filtrated, and the solvent was removed under reduced pressure. Methanol was added to the obtained residue, and solid matter was filtrated to give 2-((2-aminophenyl)amino)-4-phenethylbenzoic acid 13 mg of white solid.

Provenance & Evidence