Methanol → HCID 57667992, compound

Participants

Reaction Conditions

Reaction Steps

To a mixed solution of methanol 1.0 mL and ethyl acetate 1.0 mL of 2-(4-acetylanilino)-4-phenethylbenzoic acid 10 mg was added 5% palladium-carbon 2.0 mg at room temperature, and it was stirred under hydrogen atmosphere at 40° C. for 7 hours. After the reaction mixture was cooled to room temperature, insoluble matter was filtrated, and the solvent was removed under reduced pressure to give 2-(4-ethylanilino)-4-phenethylbenzoic acid 9.7 mg of a white solid.

Provenance & Evidence