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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2191784Generated: November 3, 2026

Ethyl Acetate → HCID 57668099, compound

https://huagongshe.com/reaction/2191784

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthyl AcetateHCID 8857—
ReactantHCID 57667858HCID 57667858—
CatalystHCID 178418390HCID 178418390—
SolventMethanolHCID 887—
ProductHCID 57668099HCID 57668099—

Reaction Steps

To the obtained 2-(4-fluoroanilino)-4-((E)-2-(3-methylphenyl)vinyl)benzoic acid, ethyl acetate 1.0 mL, methanol 1.0 mL and 10% palladium-carbon 2.0 mg were added sequentially, and it was stirred under hydrogen atmosphere at room temperature for 3 hours and 30 minutes. The solvent was removed under reduced pressure after insoluble matter was filtrated to give 2-(4-fluoroanilino)-4-(2-(3-methylphenyl)ethyl)benzoic acid 3.0 mg of a white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08327467B2
Source datasetuspto-grants-2012_12
ORD IDord-e064523d502548c4aa656f7f53577ad9
Source noteuspto-grants-2012_12