HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68962009, compound → HCID 68965243, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68962009 | HCID 68962009 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 68965243 | HCID 68965243 | — |
Reaction Steps
Trifluoroacetic acid 10 mL was added to the obtained tert-butyl 2-((benzo-1,3-dioxol-5-yl)amino)-4-(indolin-1-yl)benzoate, and it was stirred at room temperature for 2 hours. The solvent was removed under reduced pressure, methanol was added to the obtained residue, and solid matter was filtrated to give 2-((benzo-1,3-dioxol-5-yl)amino)-4-(indolin-1-yl)benzoic acid 31 mg of a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08327467B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-8922645bde074e1d9478cf4427d91c21 |
| Source note | uspto-grants-2012_12 |