HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → 2-((4-(Acetamido)phenyl)amino)-4-phenethylbenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Tert-butyl 2-((4-(acetamido)phenyl)amino)-4-phenethylbenzoate | HCID 68957261 | — |
| Product | 2-((4-(Acetamido)phenyl)amino)-4-phenethylbenzoic acid | HCID 57668063 | — |
Reaction Steps
Trifluoroacetic acid 7.5 mL was added to the obtained tert-butyl 2-((4-(acetamido)phenyl)amino)-4-phenethylbenzoate, and it was stirred at room temperature for 2 hours. The solvent was removed under reduced pressure, methanol was added to the obtained residue, and solid matter was filtrated to give 2-((4-(acetamido)phenyl)amino)-4-phenethylbenzoic acid 23 mg of a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08327467B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-b9853af598904e009feca33baf0fa0b5 |
| Source note | uspto-grants-2012_12 |