HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Nitrophenyl isocyanate → HCID 44187417, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Nitrophenyl isocyanate | HCID 76835 | — |
| Reactant | 4-Cyclopentylamino-8-methoxy-quinoline-3-carboxylic acid ethyl ester | HCID 67249718 | — |
| Product | HCID 44187417 | HCID 44187417 | 43.9% |
Reaction Steps
1-Cyclopentyl-7-methoxy-3-(3-nitro-phenyl)-1H-pyrimido[5,4-c]quinoline-2,4-dione (19 mg) was prepared from 4-cyclopentylamino-8-methoxy-quinoline-3-carboxylic acid ethyl ester (0.1 mmol) and 1-isocyanato-3-nitro-benzene (0.5 mmol) following general procedure C. LCMS: m/z 433 [M+1]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08329715B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-48f293879f594414b602f5bbe6938939 |
| Source note | uspto-grants-2012_12 |