N-1,2-Benzisoxazol-3-yl-2-chloroacetamide → HCID 86655270, compound

Participants

Reaction Steps

1-Phenyl-cycloheptanecarboxylic acid (R)-(1-aza-bicyclo[2.2.2]oct-3-yl)ester (Example 1e) (114 mg) and N-benzo[d]isoxazol-3-yl-2-chloro-acetamide (Example 4a) (89 mg) were dissolved in acetonitrile (10 mL) and left for one week. The resulting crystals were filtered off and washed with diethyl ether (3×10 mL) to afford the titled compound as a solid (120 mg).

Provenance & Evidence