Triethylamine → HCID 58149882, compound

Participants

Reaction Steps

A solution of 5-chloro-6-[(1-methylethyl)oxy]-3-pyridinecarbonyl chloride (D33; 94 mg, 0.4 mmol) in dry DMF (1.5 ml) was added to a stirred solution of 1,1-dimethylethyl 3-{5-[(hydroxyamino)(imino)methyl]-1-isoquinolinyl}propanoate (D36; 114 mg, 0.360 mmol) and triethylamine (0.084 ml, 0.600 mmol) in dry DMF (1.5 ml) at 0° and the mixture was allowed to warm to room temperature and stirred for 45 min.

Provenance & Evidence