Furfurylamine → HCID 59625312, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of ethyl 2-chloro-5,6,7,8-tetrahydroquinoline-3-carboxylate (500 mg) and furfurylamine (3.0, ml) was stirred in a sealed tube at 130° C. for 12 hr. The reaction mixture was subjected to silica gel column chromatography, and the fraction eluted with ethyl acetate-hexane (10:90-50:50) was concentrated under reduced pressure to give the object compound (683 mg).

Provenance & Evidence