Methanol → HCID 86597768, compound

Participants

Reaction Steps

A suspension of 510 mg 4-{2-fluoro-4-[(5S)-5-(methyl-sulfanylthiocarbonylamino-methyl)-2-oxo-oxazolidin-3-yl]-phenyl}-piperazine-1-carboxylic acid tert-butyl ester (1.05 mmol) in 1.25 M/methanol was stirred for 5 days. The solvent was evaporated and the residue digested in water. The water layer was neutralized at pH 7 with a saturated solution of sodium bicarbonate and evaporated to dryness. The residue was digested in CH2Cl2/MeOH. The salts were filtered and the solvent evaporated:

Provenance & Evidence