Methyl 4-iodobenzoate → HCID 59578079, compound

HRID 2194133Notes

Reaction equation

HRID 2194133 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[S:8]([N:11]1[CH2:21][CH2:20][C:14]2([C:18](=[O:19])[NH:17][CH2:16][CH2:15]2)[CH2:13][CH2:12]1)(=[O:10])=[O:9].[CH3:22][O:23][C:24](=[O:32])[C:25]1[CH:30]=[CH:29][C:28](I)=[CH:27][CH:26]=1>>[CH3:22][O:23][C:24](=[O:32])[C:25]1[CH:30]=[CH:29][C:28]([N:17]2[CH2:16][CH2:15][C:14]3([CH2:20][CH2:21][N:11]([S:8]([C:3]4[CH:4]=[CH:5][CH:6]=[CH:7][C:2]=4[Cl:1])(=[O:9])=[O:10])[CH2:12][CH2:13]3)[C:18]2=[O:19])=[CH:27][CH:26]=1

Participants

3

Reactant 2

HCID 69273Methyl 4-iodobenzoateHCID 595779948-(2-Chloro-benzenesulfonyl)-2,8-diaza-spiro[4.5]decan-1-one

Product 1

HCID 59578079HCID 59578079, compound

Procedure

This material was prepared in analogy to example 148 step F) from 8-(2-chloro-benzenesulfonyl)-2,8-diaza-spiro[4.5]decan-1-one and 4-iodo-benzoic acid methyl ester White solid. MS (ESI): 463.1 MH+).

Sources & evidence

ORD record
ord-f07242ee66144178ae78a35d2d626d80
Source dataset
uspto-grants-2012_12
Patent number
US08329904B2

Reaction notes

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