HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4-Bromophenyl)ethanol → 8-(2-Chloro-benzenesulfonyl)-2-[4-(1-hydroxy-ethyl)-phenyl]-2,8-diaza-spiro[4.5]decan-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4-Bromophenyl)ethanol | HCID 95352 | — |
| Reactant | 8-(2-Chloro-benzenesulfonyl)-2,8-diaza-spiro[4.5]decan-1-one | HCID 59577994 | — |
| Product | 8-(2-Chloro-benzenesulfonyl)-2-[4-(1-hydroxy-ethyl)-phenyl]-2,8-diaza-spiro[4.5]decan-1-one | HCID 59577982 | — |
Reaction Steps
This material was prepared in analogy to example 148 step F) from 8-(2-chloro-benzenesulfonyl)-2,8-diaza-spiro[4.5]decan-1-one and 1-(4-bromo-phenyl)-ethanol. White solid. MS (ESI): 449.1 MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08329904B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-934e8ac9e0d1473d88f4c978c15fb3ca |
| Source note | uspto-grants-2012_12 |