HCID 65488938, compound → HCID 59578008, compound

HRID 2194141Notes

Reaction equation

HRID 2194141 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[S:8]([N:11]1[CH2:22][CH2:21][C:14]2([C:19](=[O:20])[NH:18][CH2:17][CH2:16][CH2:15]2)[CH2:13][CH2:12]1)(=[O:10])=[O:9].[CH2:23]([O:25][CH2:26][C:27]1[CH:32]=[CH:31][C:30](I)=[CH:29][CH:28]=1)[CH3:24]>>[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[S:8]([N:11]1[CH2:22][CH2:21][C:14]2([C:19](=[O:20])[N:18]([C:30]3[CH:31]=[CH:32][C:27]([CH2:26][O:25][CH2:23][CH3:24])=[CH:28][CH:29]=3)[CH2:17][CH2:16][CH2:15]2)[CH2:13][CH2:12]1)(=[O:9])=[O:10]

Participants

3

Reactant 2

HCID 65488938HCID 65488938, compoundHCID 66788091HCID 66788091, compound

Product 1

HCID 59578008HCID 59578008, compound

Procedure

This material was prepared in analogy to example 158) from 9-(2-chloro-benzenesulfonyl)-2,9-diaza-spiro[5.5]undecan-1-one and 1-ethoxymethyl-4-iodo-benzene. White solid. MS (ESI): 477.4 (MH+).

Sources & evidence

ORD record
ord-bc061a7640444a2a953d8aa7272770ab
Source dataset
uspto-grants-2012_12
Patent number
US08329904B2

Reaction notes

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