HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chlorophenethylamine → HCID 59578030, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chlorophenethylamine | HCID 139381 | — |
| Reactant | Dimethylalumanylium chloride | HCID 16686359 | — |
| Reactant | 1-(2-Chloro-benzenesulfonyl)-4-(2-methoxy-ethyl)-piperidine-4-carboxylic acid ethyl ester | HCID 66787676 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 59578030 | HCID 59578030 | — |
Reaction Steps
This material was prepared in analogy to example 1 step D) from 1-(2-chloro-benzenesulfonyl)-4-(2-methoxy-ethyl)-piperidine-4-carboxylic acid ethyl ester, dimethylaluminium chloride in toluene and 2-(3-Chloro-phenyl)-ethylamine. MS (ESI): 467.2 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08329904B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-393a8e66bb1943f48d7f5f6797c38308 |
| Source note | uspto-grants-2012_12 |