HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Ethylaniline → HCID 58287273, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Ethylaniline | HCID 11504 | — |
| Reactant | Dimethylalumanylium chloride | HCID 16686359 | — |
| Reactant | 4-(2-Methoxy-ethyl)-piperidine-1,4-dicarboxylic acid 1-tert-butyl ester 4-ethyl ester | HCID 58287261 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 58287273 | HCID 58287273 | — |
Reaction Steps
This material was prepared in analogy to example 251 step A) from 4-(2-methoxy-ethyl)-piperidine-1,4-dicarboxylic acid 1-tert-butyl ester 4-ethyl ester, dimethylaluminium chloride in hexane and 4-ethyl-phenylamine, with concomitant cleavage of the Boc protecting group under the conditions. MS (ESI): 259.1 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08329904B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-2584886f0f734364acc65943dfe738ff |
| Source note | uspto-grants-2012_12 |