HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Hydroxy-4'-methoxy-2-nitrobenzanilide → 2-Amino-3-hydroxy-4'-methoxybenzanilide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Hydroxy-4'-methoxy-2-nitrobenzanilide | HCID 18001131 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-Amino-3-hydroxy-4'-methoxybenzanilide | HCID 18001107 | 93.8% |
Reaction Steps
3-Hydroxy-4′-methoxy-2-nitrobenzanilide (1.15 g) was suspended in 50 ml of methanol, 300 mg of 10% palladium-carbon powder were added and the mixture was stirred in a hydrogen atmosphere at room temperature for 1 hour. The reaction solution was filtered through Celite and washed with methanol and the filtrate was concentrated in vacuo to give 966 mg of 2-amino-3-hydroxy-4′-methoxybenzanilide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE043481E1 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-471548bf93da41dba6e084db8f058528 |
| Source note | uspto-grants-2012_06 |