HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → 4-[4-(3-chloro-phenylethynyl)-2-methyl-imidazol-1-yl]-1-ethyl-1H-pyridin-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | 4-[4-(3-chloro-phenylethynyl)-2-methyl-imidazol-1-yl]-1H-pyridin-2-one | HCID 49872574 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 4-[4-(3-chloro-phenylethynyl)-2-methyl-imidazol-1-yl]-1-ethyl-1H-pyridin-2-one | HCID 49872576 | — |
Reaction Steps
The title compound, orange gum, MS: m/e=338.3, 340.2 (M+H+), was prepared in accordance with the general method of example 2 from 4-[4-(3-chloro-phenylethynyl)-2-methyl-imidazol-1-yl]-1H-pyridin-2-one and ethyl iodide in acetone instead of DME.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08334287B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-b94e09f896734cd0bb84c007b4d92077 |
| Source note | uspto-grants-2012_12 |