3-Methylphenylacetylene → HCID 178424902, compound

HRID 2194394Notes

Reaction equation

HRID 2194394 reaction equation
I[C:2]1[NH:6][C:5]([CH3:7])=[N:4][CH:3]=1.[C:8]([C:10]1[CH:15]=[CH:14][CH:13]=[C:12]([CH3:16])[CH:11]=1)#[CH:9]>>[CH3:7][C:5]1[NH:4][CH:3]=[C:2]([C:9]#[C:8][C:10]2[CH:11]=[C:12]([CH3:16])[CH:13]=[CH:14][CH:15]=2)[N:6]=1

Participants

3

Reactant 2

HCID 1366003-MethylphenylacetyleneHCID 27946235-Iodo-2-methyl-1H-imidazole

Product 1

HCID 178424902HCID 178424902, compound

Procedure

The title compound, orange solid, MS: m/e=197.2 (M+H+) was prepared in accordance with the general method of example 1c from 5-iodo-2-methyl-1H-imidazole and 1-ethynyl-3-methyl-benzene.

Sources & evidence

ORD record
ord-70c482b7cbd54ec28c8dd2cc2c0a7f89
Source dataset
uspto-grants-2012_12
Patent number
US08334287B2

Reaction notes

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