HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 58111182, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 178432713 | HCID 178432713 | — |
| Product | HCID 58111182 | HCID 58111182 | — |
Reaction Steps
The title compound, yellow cristalline solid, MS: m/e=325.2, 327.1 (M+H+), was prepared in accordance with the general method of example 2 from 6-[4-(2-chloro-pyridin-4-ylethynyl)-2-methyl-imidazol-1-yl]-pyridin-2-ol and methyl iodide, along with the O-alkylation product from which it was separated by flash chromatography (gradient: EtOAc to EtOAc/MeOH 95:5).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08334287B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-e6c136c7f0814824aa5fe1a5773b7932 |
| Source note | uspto-grants-2012_12 |