HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methylphenylacetylene → 6-(2,5-dimethyl-4-m-tolylethynyl-imidazol-1-yl)-3-methyl-3H-pyrimidin-4-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methylphenylacetylene | HCID 136600 | — |
| Reactant | 6-(4-iodo-2,5-dimethyl-imidazol-1-yl)-3-methyl-3H-pyrimidin-4-one | HCID 66865686 | — |
| Product | 6-(2,5-dimethyl-4-m-tolylethynyl-imidazol-1-yl)-3-methyl-3H-pyrimidin-4-one | HCID 49872864 | — |
Reaction Steps
The title compound, yellow solid, MS: m/e=319.2 (M+H+), was prepared in accordance with the general method of example 1c from 6-(4-iodo-2,5-dimethyl-imidazol-1-yl)-3-methyl-3H-pyrimidin-4-one and 1-ethynyl-3-methyl-benzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08334287B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-b777b3bb6ffe45d595ad33f28fa50ed8 |
| Source note | uspto-grants-2012_12 |