HCID 66864934, compound → 2-ethyl-5-(4-iodo-2-methyl-imidazol-1-yl)-2H-pyridazin-3-one
Reaction equation
Cl[C:2]1[CH:7]=[N:6][N:5]([CH2:8][CH3:9])[C:4](=[O:10])[CH:3]=1.[I:11][C:12]1[N:13]=[C:14]([CH3:17])[NH:15][CH:16]=1>>[CH2:8]([N:5]1[C:4](=[O:10])[CH:3]=[C:2]([N:15]2[CH:16]=[C:12]([I:11])[N:13]=[C:14]2[CH3:17])[CH:7]=[N:6]1)[CH3:9]Participants
3
Procedure
The title compound, white crystalline solid, MS: m/e=331.0 (M+H+), was prepared in accordance with the general method of example 23b from 5-chloro-2-ethyl-2H-pyridazin-3-one and 4-Iodo-2-methyl-1H-imidazole.
Sources & evidence
- ORD record
- ord-fb2763ff85b44113846f770ec294e771
- Source dataset
- uspto-grants-2012_12
- Patent number
- US08334287B2
Reaction notes
Loading…