Sodium Methoxide → HCID 66865809, compound

HRID 2194462Notes

Reaction equation

HRID 2194462 reaction equation
[Cl:1][C:2]1[C:3](=[O:13])[N:4]([CH2:9][CH2:10][O:11][CH3:12])[N:5]=[CH:6][C:7]=1Cl.[CH3:14][O-:15].[Na+]>CO>[Cl:1][C:2]1[C:3](=[O:13])[N:4]([CH2:9][CH2:10][O:11][CH3:12])[N:5]=[CH:6][C:7]=1[O:15][CH3:14]

Participants

4

Reactant 2

HCID 10942334Sodium MethoxideHCID 66864935HCID 66864935, compound

Product 1

HCID 66865809HCID 66865809, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The title compound, white crystalline solid, MS: m/e=219.1, 221.1 (M+H+), was prepared in accordance with the general method of example 23e by treatment of 4,5-dichloro-2-(2-methoxy-ethyl)-2H-pyridazin-3-one with sodium methoxide in methanol.

Sources & evidence

ORD record
ord-f8d07c5c88f64ba38f596d9e07f31bbf
Source dataset
uspto-grants-2012_12
Patent number
US08334287B2

Reaction notes

Loading…