HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2194526Generated: November 1, 2026
(2-Anilinopyridin-3-yl)methanol → HCID 13983610, compound
https://huagongshe.com/reaction/2194526
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | (2-Anilinopyridin-3-yl)methanol | HCID 13986159 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 13983610 | HCID 13983610 | 104.7% |
Reaction Steps
6.35 g (31.7 mmol) of (2-phenylamino-3-pyridinyl)methanol was dissolved in chloroform (100 mL), and 8.27 g (95.1 mmol) of manganese dioxide was added thereto. The resulting mixture was stirred for 7 hours at 60° C. The reaction mixture was filtered, and the filtrate was concentrated. Thus, 6.58 g of the title compound was obtained as an orange-colored solid (yield: quantitative).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08334236B2 |
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| Source dataset | uspto-grants-2012_12 |
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| ORD ID | ord-6eb5ed50435d4adc87613fed18464197 |
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| Source note | uspto-grants-2012_12 |
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