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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2194526Generated: November 1, 2026

(2-Anilinopyridin-3-yl)methanol → HCID 13983610, compound

https://huagongshe.com/reaction/2194526

Reaction equation

Participants

RoleNameHCIDCharge
Reactant(2-Anilinopyridin-3-yl)methanolHCID 13986159—
CatalystHCID 178418406HCID 178418406—
SolventChloroformHCID 6212—
ProductHCID 13983610HCID 13983610104.7%

Reaction Conditions

Temperature60 °C

Reaction Steps

6.35 g (31.7 mmol) of (2-phenylamino-3-pyridinyl)methanol was dissolved in chloroform (100 mL), and 8.27 g (95.1 mmol) of manganese dioxide was added thereto. The resulting mixture was stirred for 7 hours at 60° C. The reaction mixture was filtered, and the filtrate was concentrated. Thus, 6.58 g of the title compound was obtained as an orange-colored solid (yield: quantitative).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08334236B2
Source datasetuspto-grants-2012_12
ORD IDord-6eb5ed50435d4adc87613fed18464197
Source noteuspto-grants-2012_12