Cesium carbonate → HCID 58203520, compound

Participants

Reaction Steps

To a mixture of 5-isopropyl-2,6-dimethoxy-pyrimidin-4-ol (64 mg, 0.322 mmol) and N-phenyltrifluoromethane sulfonamide (127 mg, 1.1 eq.) in 3 mL of DCM, Cs2CO3 (116 mg, 1.1 eq.) was added. The reaction mixture was stirred at room temperature for 90 minutes. The reaction mixture was concentrated down and purified (silica gel, 0-80% EtOAC/hexane) to give white solid (74 mg, 69%). LC-MS shows 330.9 (M+1).

Provenance & Evidence