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HRID2194889

反应详情

EQUATION

反应方程式

HRID 2194889 的结构方程式

REACTANTS

反应物

2
结构：N#CCc1ccc(Br)cc1
HCID27914

4-Bromophenylacetonitrile

C8H6BrN

结构：Cc1cc(Cl)c(OCCOc2ccc(CBr)cc2)c(Cl)c1
HCID58488438

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(Cl)c(OCCOc2ccc(CC(C#N)c3ccc(Br)cc3)cc2)c(Cl)c1
HCID67449101

未命名化合物

PROCEDURE

实验过程

Prepared according to the procedure described in EXAMPLE 1, step 4 using commercially available (4-bromophenyl)acetonitrile and 1,3-dichloro-2-{2-[4-(bromomethyl)phenoxy]ethoxy}-5-methylbenzene (II.2) as starting materials. Purification by column chromatography on silica gel, eluting with Hex/EtOAc 15%, afforded the desired compound as a colorless oil.

WORKUP

后处理

  1. customPrepared
  2. customPurification by column chromatography on silica gel
  3. washeluting with Hex/EtOAc 15%