HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 11243735, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 68510891 | HCID 68510891 | — |
| Product | HCID 11243735 | HCID 11243735 | — |
Reaction Steps
A mixture of 3-tert-butyl-8-methoxy-2-methyl-4-phenylisoquinolin-1(2H)-one (0.500 g) and 48% HBr (15 mL) was heated at reflux overnight. The reaction was concentrated and purified by flash chromatography (10% EtOAc in hexanes) to give the titled compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08338449B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-ca1de38f079b40a2a732dc936145b878 |
| Source note | uspto-grants-2012_12 |