Trifluoroacetic acid → HCID 59354994, compound

Participants

Reaction Steps

The title compound was prepared as a white solid according to the procedure of Example 43, except substituting N-{(1S)-2-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-1-[(3-fluorophenyl)methyl]ethyl}-4-(1-methyl-1H-1,2,3-triazol-5-yl)benzamide for N-((1S)-2-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-1-{[2-(trifluoromethyl)phenyl]methyl}ethyl)-4-(1-methyl-1H-1,2,3-triazol-5-yl)benzamide. The title compound was a TFA salt: LC-MS (ES) m/z 354.2 (M+H)+, 1H NMR (400 MHz, MeOD) δ ppm 7.94-7.90 (m, 3H), 7.69 (m, 2H), 7.33 (m, 1H) 7.15-7.07 (m, 2H), 6.98 (m, 1H), 4.62 (m, 1H), 4.15 (s, 3H), 3.30-2.96 (m, 4H).

Provenance & Evidence