Ethyl bromoacetate → HCID 86652071, compound

HRID 2196446Notes

Reaction equation

[Br:1][C:2]1[CH:3]=[CH:4][C:5]([NH2:8])=[N:6][CH:7]=1.Br[CH2:10][C:11]([O:13][CH2:14][CH3:15])=[O:12]>>[BrH:1].[Br:1][C:2]1[CH:3]=[CH:4][C:5](=[NH:8])[N:6]([CH2:10][C:11]([O:13][CH2:14][CH3:15])=[O:12])[CH:7]=1

Participants

Reactant 2

HCID 7748Ethyl bromoacetate

HCID 706222-Amino-5-bromopyridine

Product 1

HCID 86652071HCID 86652071, compound

Procedure

By carrying out the process as in Example 3.1 and using 5.0 g of 5-bromopyridin-2-ylamine and 9.6 ml of ethyl 2-bromoacetate, 9.56 g of compound are obtained.

Workup

customare obtained

Sources & evidence

ORD record: ord-e6bd930df6894e54a2b4d00e4640bb0d
Source dataset: uspto-grants-2012_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08338451B2

Reaction notes

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