HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 86620757, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 15-Crown-5 | HCID 36336 | — |
| Reactant | 2-Chloropyridine-3-sulfonyl chloride | HCID 10219968 | — |
| Reactant | 5-Phenyl-1H-pyrrole-3-carboxaldehyde | HCID 11052090 | — |
| Product | HCID 86620757 | HCID 86620757 | — |
Reaction Steps
By a reaction under similar conditions as in Reference Example 55 and using 5-phenyl-1H-pyrrole-3-carbaldehyde (514 mg), sodium hydride (60% in oil, 180 mg), 15-crown-5 (0.90 mL) and 2-chloro-3-pyridinesulfonyl chloride (716 mg), the title compound was obtained as an amorphous form (yield 716 mg, 69%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08338461B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-3ca73ed37e054906a70652ef74c4f904 |
| Source note | uspto-grants-2012_12 |