Propionic Acid → HCID 178437978, compound

HRID 219715Notes

Reaction equation

HRID 219715 reaction equation
[CH3:1][N:2]1[C:6]([CH2:7]OC)=[N:5][N:4]=[C:3]1[SH:10].[C:11](O)(=O)CC.CNC(=S)NN>>[CH3:1][N:2]1[C:6]([CH2:7][CH3:11])=[N:5][N:4]=[C:3]1[SH:10]

Participants

4

Reactant 3

HCID 1032Propionic AcidHCID 2723853N-MethylhydrazinecarbothioamideHCID 178494712HCID 178494712, compound

Product 1

HCID 178437978HCID 178437978, compound

Procedure

The reaction was performed similar to the method described for the preparation 4-Methyl-5-methoxymethyl-4H-[1,2,4]triazole-3-thiol by reacting 16.4 g of N,N′-carbonyldiimidazol (0.101 mol) with 5 g of propionic acid (0.067 mol) and 14.2 g of 4-methyl-3-thiosemicarbazid (0.135 mol). Yield: 3.8 g

Sources & evidence

ORD record
ord-73691a648ee24ae5b8c8e3d41b1bff17
Source dataset
uspto-grants-2012_06
Patent number
US08202868B2

Reaction notes

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