HCID 67498612, compound → HCID 67499593, compound

HRID 2197586Notes

Reaction equation

HRID 2197586 reaction equation
[F:1][C:2]1([C:12]2[C:17]([CH3:18])=[CH:16][CH:15]=[CH:14][N:13]=2)[CH2:11][CH2:10][C:5]2(OCC[O:6]2)[CH2:4][CH2:3]1.ClC1C(C2(F)CCC3(OCCO3)CC2)=NC=CC=1>>[F:1][C:2]1([C:12]2[C:17]([CH3:18])=[CH:16][CH:15]=[CH:14][N:13]=2)[CH2:11][CH2:10][C:5](=[O:6])[CH2:4][CH2:3]1

Participants

3

Reactant 2

HCID 67498612HCID 67498612, compoundHCID 67499172HCID 67499172, compound

Product 1

HCID 67499593HCID 67499593, compound

Procedure

The title compound was prepared using the procedure as described in Example 1C, except for substituting the product of Example 10B for the product of Example 1B. 1H NMR (300 MHz, DMSO-d6) δ ppm 8.37 (d, J=4.4 Hz, 1 H) 7.66 (d, J=6.8 Hz, 1 H) 7.29 (dd, J=6.8, 4.4 Hz, 1 H), 2.54-2.93 (m, 4 H), 2.51 (s, 3 H), 2.18-2.46 (m, 4 H). MS (DCI) m/e 208 (M+H)+.

Sources & evidence

ORD record
ord-1c780babd0ba482e90ed6303c4630904
Source dataset
uspto-grants-2012_12
Patent number
US08338603B2

Reaction notes

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