HCID 67499044, compound → HCID 67499337, compound

HRID 2197588Notes

Reaction equation

HRID 2197588 reaction equation
[F:1][C:2]1([C:12]2[S:13][CH:14]=[CH:15][N:16]=2)[CH2:11][CH2:10][C:5]2(OCC[O:6]2)[CH2:4][CH2:3]1.ClC1C(C2(F)CCC3(OCCO3)CC2)=NC=CC=1>>[F:1][C:2]1([C:12]2[S:13][CH:14]=[CH:15][N:16]=2)[CH2:3][CH2:4][C:5](=[O:6])[CH2:10][CH2:11]1

Participants

3

Reactant 2

HCID 67499044HCID 67499044, compoundHCID 67499172HCID 67499172, compound

Product 1

HCID 67499337HCID 67499337, compound

Procedure

The title compound was prepared using the procedure as described in Example 1C, except for substituting the product of Example 20B for the product of Example 1B. 1HNMR (300 MHz, DMSO-d6) δ ppm 7.82-7.95 (m, 2 H), 2.61-2.72 (m, 6 H), 2.24-2.42 (m, 2 H). MS (DCI) m/e 200 (M+H)+.

Sources & evidence

ORD record
ord-420764d48adc423bbdddcfa65ee2bd88
Source dataset
uspto-grants-2012_12
Patent number
US08338603B2

Reaction notes

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