Stannous Chloride → HCID 61244331, compound
Reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][C:9]2[CH:10]=[C:11]([CH3:15])[CH:12]=[CH:13][CH:14]=2)=[C:4]([N+:16]([O-])=O)[CH:3]=1.Cl[Sn]Cl>>[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][C:9]2[CH:10]=[C:11]([CH3:15])[CH:12]=[CH:13][CH:14]=2)=[C:4]([NH2:16])[CH:3]=1Participants
3
Procedure
The product from Example 48a was reduced with SnCl2 following the procedure from Example 1f giving the title compound.
Sources & evidence
- ORD record
- ord-73b8e322b1f74ead8a1f15796ec1ffca
- Source dataset
- uspto-grants-2012_12
- Patent number
- US08338605B2
Reaction notes
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