HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-2-methyl-1,8-naphthyridine → HCID 68460795, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-2-methyl-1,8-naphthyridine | HCID 12266372 | — |
| Reactant | HCID 68458106 | HCID 68458106 | — |
| Product | HCID 68460795 | HCID 68460795 | — |
Reaction Steps
The product from Example 1d (2.06 g, 1.16 mmol) was reacted with the Product from Example 53b (3.18 g, 1.16 mmol) for 5 h following the procedure from Example 1g giving the crude title compound which was purified by HPLC with TFA providing the trifluoroacetic acid salt (3.61 g, 59%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08338605B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-36338175e35b4857b7e95b5108a53af7 |
| Source note | uspto-grants-2012_12 |